(E)-4-二乙氧基磷酰丁-2-烯醛合成路线 （共 7 条）
反应条件
chromium(VI) oxide; sulfuric acid in acetone T=0°C; 0.25 h;
参考文献
Kann, Nina; Rein, Tobias; Akermark, Bjoern; Helquist, Paul
Journal of Organic Chemistry, 1990 , vol. 55, # 19 p. 5312 - 5323
反应条件
jones reagent in acetone T=0°C; 0.75 h;
参考文献
Rein, Tobias; Aekermark, Bjoern; Helquist, Paul
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 8 p. 569 - 572
反应条件
in toluene 16 h; Heating;
参考文献
Oehler, Elisabeth; Kang, Heun-Soo; Zbiral, Erich
Chemische Berichte, 1988 , vol. 121, p. 299 - 308
反应条件
cyclohexylamine; lithium diisopropyl amide in tetrahydrofuran T=0 - 25°C; 2 h;
参考文献
Kann, Nina; Rein, Tobias; Akermark, Bjoern; Helquist, Paul
Journal of Organic Chemistry, 1990 , vol. 55, # 19 p. 5312 - 5323
反应条件
cyclohexylamine; lithium diisopropyl amide in tetrahydrofuran T=0 - 25°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 19 p. 5312 - 5323
反应条件
Caprylic Aldehyde; lithium diisopropyl amide in tetrahydrofuran T=0 - 25°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 19 p. 5312 - 5323
反应条件
1: molecular sieves / tetrahydrofuran / Ambient temperature
2: LDA / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 25 deg C, 111 h
View Scheme
参考文献
Rein, Tobias; Aekermark, Bjoern; Helquist, Paul
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 8 p. 569 - 572
