(2-溴甲基)-4-甲基-1-硝基苯合成路线 (共 2 条)
反应条件
phosphorus tribromide in dichloromethane T=20°C; 0.5 h;
参考文献
UNIVERSITY OF UTAH RESEARCH FOUNDATION; JI, Haitao; YU, Binxun; ZHANG, Min; GUO, Wenxing
Patent: WO2013/120045 A1, 2013 ;
Location in patent: Paragraph 00273 ;
反应条件
1: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 80 °C / |Inert atmosphere 2: phosphorus tribromide / diethyl ether / 3 h / |Inert atmosphere View Scheme
参考文献
UNIVERSITY OF UTAH RESEARCH FOUNDATION; JI, Haitao; YU, Binxun; ZHANG, Min; GUO, Wenxing
Patent: WO2013/120045 A1, 2013 ;