反应条件
in tetrahydrofuran
byproducts: NaCl, H2; Ar-atmosphere; stirring of UCl4, COT and NaH (24 h, room temp.); addn. of excess TMEDA, stirring (1 h), filtration, evapn. (vac.), heating of residue (vac., several h), extn. (hexane, 18 h), drying (several h);
参考文献
Boussie, Thomas R.; Moore, Robert M. Jr.; Streitwieser, Andrew; Zalkin, Alan; Brennan, John; Smith, Kennith A.
Organometallics, 1990 , vol. 9, p. 2010 - 2016