α,α,α'-三(4-羟苯基)-1-乙基-4-异丙苯合成路线 （共 5 条）
反应条件
hydrogenchloride; lauryl mercaptan in toluene T=45 - 50°C; 22.5 h; Inert atmosphere;
参考文献
HONSHU CHEMICAL INDUSTRY CO., LTD.
Patent: US2012/108853 A1, 2012 ;
Location in patent: Page/Page column 16-17 ;
反应条件
hydrogenchloride; lauryl mercaptan in toluene T=40 - 45°C; 21 h; Inert atmosphere;
参考文献
US2012/108853 A1, ;
Page/Page column 15 ;
反应条件
1.1: AlCl3, aluminium chloride / chloroform / 1 h / 5 °C / Inert atmosphere 1.2: 5 h / 5 - 20 °C 1.3: 1 h / 30 °C 2.1: hydrogenchloride; lauryl mercaptan / toluene / 22.5 h / 45 - 50 °C / Inert atmosphere View Scheme
反应条件
1.1: AlCl3, aluminium chloride / dichloromethane / 1.5 h / 5 - 10 °C / Inert atmosphere 1.2: 4.5 h / 5 - 10 °C 1.3: 0.5 h / 30 °C 2.1: sodium hydroxide; water / toluene; methanol / 2 h / 50 °C 3.1: hydrogenchloride; lauryl mercaptan / toluene / 21 h / 40 - 45 °C / Inert atmosphere View Scheme
反应条件
1: sodium hydroxide; water / toluene; methanol / 2 h / 50 °C 2: hydrogenchloride; lauryl mercaptan / toluene / 21 h / 40 - 45 °C / Inert atmosphere View Scheme
