1,1,3,3-四苯基-1,3-二硅氧烷二醇合成路线 (共 25 条)
参考文献
Kipping
Journal of the Chemical Society, 1912 , vol. 101, p. 2108
参考文献
Kipping; Robison
Journal of the Chemical Society, 1914 , vol. 105, p. 487
反应条件
pyridine in toluene 3 h; Heating;
参考文献
Achelashvili, V. A.; Mukbaniani, O. V.; Khananashvili, L. M.; Kikoladze, V. S.; Tsitsishvili, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1530 - 1535,1355 - 1359
反应条件
pyridine in toluene 3 h; Heating;
参考文献
Meladze, S. M.; Mukbaniani, O. V.; Khananashvili, L. M.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 7 p. 1624 - 1628,1382 - 1385
反应条件
in benzene byproducts: water; refluxing (equimolar mixture, 4 h, continuous removal of water); cooling, filtration, distn. (reduced pressure), recrystn. (Et2O:petroleum ether 1:3); elem. anal.;
参考文献
Brisdon, Brian J.; Mahon, Mary F.; Molloy, Kieran C.; Schofield, Paul J.
Journal of Organometallic Chemistry, 1992 , vol. 436, # 1 p. 11 - 22