N-(3-甲氧基苯乙基)甲酰胺合成路线 (共 10 条)
参考文献
Augelli-Szafran, Corinne Elizabeth; Boehme, Thomas; Schwarz, Roy Douville
Patent: US2003/220335 A1, 2003 ;
Location in patent: Page/Page column 3-5 ;
反应条件
in toluene 6 h; Heating;
参考文献
Rohloff; Dyson; Gardner; Alfredson; Sparacino; Robinson III
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1935 - 1938
反应条件
in formic acid ethyl ester
参考文献
NIPPON SHINYAKU COMPANY, LIMITED
Patent: EP897923 A1, 1999 ;
反应条件
T=0°C; 12.5 h; Reflux;
参考文献
Wang, Zhi-Xia; Chen, Jing-Lei; Qiao, Chunhua
Chemical Biology and Drug Design, 2013 , vol. 82, # 2 p. 216 - 225
反应条件
1: 2 percent Chromat. / POCl3 2: 58 percent / aq. HCl View Scheme
参考文献
Euerby, Melvin R.; Waigh, Roger D.
Journal of Chemical Research, Miniprint, 1987 , # 2 p. 501 - 526
反应条件
1: POCl3 / 1,2,3,4-tetrahydro-naphthalene 2: dioxane / Heating View Scheme
参考文献
Augelli-Szafran, Corinne E.; Jaen, Juan C.; Moreland, David W.; Nelson, Carrie B.; Penvose-Yi, Jan R.; Schwarz, Roy D.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 15 p. 1991 - 1996
反应条件
1: 19 percent / POCl3 2: 1.) NaBH4, 2.) HCl View Scheme
参考文献
Euerby, Melvin R.; Waigh, Roger D.
Journal of Chemical Research, Miniprint, 1987 , # 2 p. 501 - 526
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 501 - 526
反应条件
triethylamine; trichlorophosphate in dichloromethane
T=-10°C; 3 h; Inert atmosphere;
参考文献
Wang, Zhi-Xia; Chen, Jing-Lei; Qiao, Chunhua
Chemical Biology and Drug Design, 2013 , vol. 82, # 2 p. 216 - 225
反应条件
1: phosphorus oxychloride / 0 °C / dann auf dem Wasserbad
2: benzene
3: zinc; concentrated hydrochloric acid
View Scheme
参考文献
Gulland; Virden
Journal of the Chemical Society, 1929 , p. 1798