1: With palladium diacetate T=130°C; 2 h; Inert atmosphereSchlenk technique; 2: With potassium hydroxide in diethyl ether; water
参考文献
Adam, Mohamed Shaker S.; Mohamad, Ahmad Desoky; Jones, Peter G.; Kindermann, Markus K.; Heinicke, Joachim W.
Polyhedron, 2013 , vol. 50, # 1 p. 101 - 111
1: 1,3-diphenyl-2-propenyl acetate With (R)-(S)-Josiphos; bis(dibenzylideneacetone)-palladium(0) in benzene 0.5 h; 2: bis-diphenylphosphine in benzene T=40°C; 48 h; optical yield given as percent eeenantioselective reaction;
参考文献
Butti, Pietro; Rochat, Raphael; Sadow, Aaron D.; Togni, Antonio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4878 - 4881
1: With palladium diacetate T=130°C; 2.5 h; Inert atmosphereSchlenk technique; 2: With sodium hydroxide in diethyl ether; water
参考文献
Adam, Mohamed Shaker S.; Mohamad, Ahmad Desoky; Jones, Peter G.; Kindermann, Markus K.; Heinicke, Joachim W.
Polyhedron, 2013 , vol. 50, # 1 p. 101 - 111
1: 1,3-diphenyl-2-propenyl acetate With (R)-(S)-Josiphos; bis(dibenzylideneacetone)-palladium(0) in dichloromethane 0.5 h; 2: bis-diphenylphosphine in dichloromethane T=40°C; optical yield given as percent eeenantioselective reaction;
参考文献
Butti, Pietro; Rochat, Raphael; Sadow, Aaron D.; Togni, Antonio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4878 - 4881
1: 3-hydroxy-1,3-diphenyl-prop-1-ene With (R)-(S)-Josiphos; bis(dibenzylideneacetone)-palladium(0) in benzene 0.5 h; 2: bis-diphenylphosphine in benzene T=40°C; optical yield given as percent eeenantioselective reaction;
参考文献
Butti, Pietro; Rochat, Raphael; Sadow, Aaron D.; Togni, Antonio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4878 - 4881
1: C17H22O2 With (R)-(S)-Josiphos; bis(dibenzylideneacetone)-palladium(0) in benzene 0.5 h; 2: bis-diphenylphosphine in benzene T=40°C; optical yield given as percent eeenantioselective reaction;
参考文献
Butti, Pietro; Rochat, Raphael; Sadow, Aaron D.; Togni, Antonio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4878 - 4881
