1: 4-iodophenyl triflate With isopropylmagnesium chloride in tetrahydrofuran T=-20°C; 2: [(Cyanocarbonyl)oxy]ethane Further stages.;
参考文献
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
1: With lithium tri-n-butylzincate in tetrahydrofuran; hexane
T=-85°C; Metallation; 0.5 h;
2: With hydrogenchloride in tetrahydrofuran; hexane
Hydrolysis;
参考文献
Harada, Toshiro; Chiba, Minako; Oku, Akira
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8210 - 8213
1: With isopropylmagnesium chloride in tetrahydrofuran
T=-20°C;
2: With 1,2,2-trichloro-1,1,2-trichloro-ethane
Further stages.;
参考文献
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
