1,10-菲咯啉-2-甲腈; 邻菲咯啉-2-甲腈合成路线 （共 11 条）
参考文献
Engbersen; Koudijs; Joosten; Van der Plas
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 989 - 900
反应条件
benzoyl chloride in water T=20°C; 1 h;
参考文献
Ryan, Patrick E.; Guenee, Laure; Piguet, Claude
Dalton Transactions, 2013 , vol. 42, # 31 p. 11047 - 11055
反应条件
1: 92 percent / 30percent H2O2 / acetic acid / 1.) 72 deg C, 6 h, 2.) room temperature, overnight; 2: 92 percent / benzoyl chloride View Scheme
参考文献
Akerboom, Sebastiaan; Van Den Elshout, Jos J. M. H.; Mutikainen, Ilpo; Siegler, Maxime A.; Fu, Wen Tian; Bouwman, Elisabeth
European Journal of Inorganic Chemistry, 2013 , # 36 p. 6137 - 6146
反应条件
acetic anhydride 2 h; Reflux;
参考文献
Zhang, Min; Gao, Rong; Hao, Xiang; Sun, Wen-Hua
Journal of Organometallic Chemistry, 2008 , vol. 693, # 26 p. 3867 - 3877
反应条件
hydrogenchloride T=90°C; 6 h;
参考文献
Ten Brink, Gerd-Jan; Arends, Isabel W. C. E.; Hoogenraad, Marcel; Verspui, Goeran; Sheldon, Roger A.
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 12 p. 1341 - 1352
反应条件
1.1: sodium / 0.5 h / Heating 1.2: 62 percent / aq. HCl / 0.5 h / 0 °C 2.1: 91 percent / sodium borohydride / ethanol / 48 h / 20 °C 3.1: 71 percent / selenium dioxide / dioxane / 2 h / Heating View Scheme
参考文献
Weijnen, John G. F.; Koudijs, Arie; Engbersen, Johan F. J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1121 - 1126
反应条件
1: With sodium
0.5 h; Reflux;
2: With hydrogenchloride in water
T=0°C; 0.5 h;
参考文献
Akerboom, Sebastiaan; Van Den Elshout, Jos J. M. H.; Mutikainen, Ilpo; Siegler, Maxime A.; Fu, Wen Tian; Bouwman, Elisabeth
European Journal of Inorganic Chemistry, 2013 , # 36 p. 6137 - 6146
反应条件
1.1: sodium / 0.5 h / Heating
1.2: 62 percent / aq. HCl / 0.5 h / 0 °C
2.1: 91 percent / sodium borohydride / ethanol / 48 h / 20 °C
View Scheme
参考文献
Weijnen, John G. F.; Koudijs, Arie; Engbersen, Johan F. J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1121 - 1126
反应条件
1: in toluene
T=70°C;
2: With (ethylenedinitrilo)tetraacetic acid disodium salt in water
参考文献
Pelletier, Jeremie D.A.; Champouret, Yohan D.M.; Cadarso, Jesus; Clowes, Lucy; Ganete, Marcos; Singh, Kuldip; Thanarajasingham, Vakesan; Solan, Gregory A.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 19 p. 4114 - 4123
反应条件
1: 86 percent / NH2NH2 / H2O; ethanol / 3 h / 20 °C
2: 80 percent / ethanol / 3 h / Heating
View Scheme
参考文献
Chao; Yang; Xue; Li; Zang; Williams; Ji; Chen
Journal of the Chemical Society, Dalton Transactions, 2001 , # 8 p. 1326 - 1331
