1-(4-甲氧基苯基)-1H-吡咯-2,5-二酮合成路线 （共 13 条）
反应条件
tetrabutylammomium bromide; sodium carbonate; dimethyl sulfate in water; 1,2-dichloro-ethane T=20°C; 10 h;
参考文献
Deshpande, Sunita R.; Maybhate, Shailaja P.; Likhite, Anjali P.; Chaudhary, Preeti M.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 4 p. 487 - 488
反应条件
1: in tetrahydrofuran T=20°C; 0.5 h; 2: With sodium acetate; acetic anhydride T=120°C; 0.5 h; Microwave irradiation; 3: With sodium hydroxide in water
参考文献
Guo, Song; Zhang, Hongli; Huang, Ling; Guo, Zhendong; Xiong, Guang; Zhao, Jianzhang
Chemical Communications, 2013 , vol. 49, # 77 p. 8689 - 8691
反应条件
1: chloroform / 1 h / 20 °C 2: sodium acetate; acetic anhydride / 2 h / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 9 p. 2823 - 2834
反应条件
triethylamine in tetrahydrofuran 3 h;
参考文献
Gaina, Constantin; Gaina, Viorica
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 655 - 661
反应条件
thionyl chloride; triethylamine in tetrahydrofuran T=20°C; 6.5 h; Reflux;
参考文献
Faturaci, Yeliz; Coskun, Necdet
Turkish Journal of Chemistry, 2012 , vol. 36, # 5 p. 749 - 758
反应条件
sodium acetate; acetic anhydride T=100°C;
参考文献
Chemistry - A European Journal, , vol. 16, # 42 p. 12534 - 12537
反应条件
tetrabutylammomium bromide in neat (no solvent, solid phase) MillingGreen chemistry;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 52, # 8 p. 1166 - 1171
反应条件
phosphorous pentoxide 1.) 0-5 deg C, 2.) RT, 4 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 39, # 9 p. 1475 - 1485
反应条件
hydrogenchloride; steam; acetic acid
参考文献
Kretow; Kul'tschizkaja
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 208,211
engl.Ausg., 1956 , vol. 26, p. 221,223
Full Text Show Details
Roderick
Journal of the American Chemical Society, 1957 , vol. 79, p. 1710
反应条件
bis-triphenylphosphine-palladium(II) chloride; 4-bromooctafluorobutanetriethoxysilane; (Z)-N,N-diisopropyl-2-styrylbenzamide in tetrahydrofuran
T=65°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Bai, Xing-Feng; Xu, Li-Wen; Zheng, Long-Sheng; Jiang, Jian-Xiong; Lai, Guo-Qiao; Shang, Jun-Yan
Chemistry - A European Journal, 2012 , vol. 18, # 26 p. 8174 - 8179
