反应条件
in tetrahydrofuran; diethyl ether soln. of CH3MgBr in diethyl ether added dropwise to soln. of Ph2SnCl2 inTHF at -78°C, warmed to ambient temp., stirred for 2 h; satd. aq. NH4Cl added, extracted with diethyl ether, combined org. phases dried over MgSO4, filtered, concd. under vac.; elem. anal.;
参考文献
Helliwell, Madeleine; Thomas, Eric J.; Townsend, Linda A.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1286 - 1296
