反应条件
1: 1.) n-BuLi / 1.) Et2O, hexane, RT, 2.) Et2O, hexane, RT 2: NaN3, CF3COOH / CHCl3 / 0 - 20 °C 3: LiAlH4 / tetrahydrofuran; diethyl ether / Ambient temperature 4: 2.) K2CO3 / 1.) DMF, 60 deg C, 48 h, 2.) DMF, heating, 24 h View Scheme
参考文献
Costa, Brian de; George, Clifford; Dominguez, Celia
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1671 - 1680
