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I.G. Farbenind.
Patent: DE467728 ;
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1: 1-ethynyl-cyclohexan-1-ol With ethylmagnesium bromide in tetrahydrofuran T=23 - 80°C; 2: cyclohexanone in tetrahydrofuran T=23 - 25°C; 3: With ammonium chloride in tetrahydrofuran; water
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1: acetylene With potassium tert-butylate in tetrahydrofuran 0.25 h; Inert atmosphere; 2: cyclohexanone in tetrahydrofuran T=20°C; 18.67 h; Inert atmosphere;
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Chemistry - A European Journal, 2010 , vol. 16, # 3 p. 760 - 765
1: trans-1,2-dichloroethylene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: cyclohexanone in tetrahydrofuran; hexane T=0°C; 3: cyclohexanone Further stages;
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