双(1-甲基-2-羟乙基)醚合成路线 (共 7 条)
反应条件
hydrogen; oxygen; palladium on activated charcoal in methanol; water T=60°C; P=15514.9 Torr; Product distribution / selectivity;
参考文献
US7238817 B1, ;
Page/Page column 6-7 ;
反应条件
titanium silicate; hydrogen; oxygen in methanol; water T=60°C; P=16274.9 Torr; 18 h; Ammonium phosphate buffer; Product distribution / selectivity;
参考文献
US2007/93668 A1, ;
Page/Page column 4-5 ;
反应条件
1: With sodium methylate T=210 - 220°C; 3 h; 2: With citric acid
参考文献
US2008/103340 A1, ;
Page/Page column 11-14 ;
反应条件
hydrogen; oxygen; Pd/TS-1 in water T=60°C; P=16274.9 Torr; pH=6; ammonium phosphate buffer; Product distribution / selectivity;
参考文献
US2007/173655 A1, ;
Page/Page column 4 ;
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4357
反应条件
oxygen T=90°C; atmospheric pressure,; Mechanism;
参考文献
Janik, R.; Gerhardt, W.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 4 p. 611 - 616
反应条件
1: triethylamine / di-isopropyl ether
2: lithium bromide / acetone / |Reflux
View Scheme
参考文献
JANSSEN RandD IRELAND; TAHRI, Abdellah; VENDEVILLE, Sandrine Marie Helene; JONCKERS, Tim Hugo Maria; RABOISSON, Pierre Jean-Marie Bernard; HU, Lili; DEMIN, Samuël Dominique; COOYMANS, Ludwig Paul
Patent: WO2014/60411 A1, 2014 ;