trimethylaluminum 1.) THF, 25 deg C, 1 h, 2.) THF, hexane, from -15 deg C to 25 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wright, Marcus W.; Smalley Jr., Terrence L.; Welker, Mark E.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1994 , vol. 116, # 15 p. 6777 - 6791