6-甲氧基-1-萘满酮合成路线 (共 219 条)
反应条件
1: 1.) BuLi / 1.) hexane, THF, -78 deg C, 3 h, 2.) -78 deg C, 4 h 2: silver triflate / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
反应条件
polyphosphoric ester in chloroform 7 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
sodium hydroxide in tetrahydrofuran 22 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2856 - 2876
反应条件
sodium hydroxide in tetrahydrofuran 22 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2856 - 2876
反应条件
tert-butyl-tetramethyl-guanidine; iodine in toluene 0.25 h; Ambient temperaturevariation of solvent and base, optimize the yield of iodide; Product distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 15 p. 1605 - 1608
反应条件
anhydrous magnesium carbonate in water; acetone 22 h; Heating;
参考文献
Bhattacharya, S.; Mandal, A. N.; Chaudhuri, S. R. Ray; Chatterjee, A.
Tetrahedron Letters, 1984 , vol. 25, # 28 p. 3007 - 3010
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4163 - 4164
反应条件
acetic anhydride zuletzt unter Eindampfen im Hochvakuum;
参考文献
Journal of the Chemical Society, , p. 68,70
反应条件
2,4,6-trimethyl-pyridine
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 540 - 550
反应条件
1: amalgamated zinc; aqueous hydrochloric acid 2: concentrated sulfuric acid View Scheme
参考文献
Journal of the Chemical Society, , p. 2310,2313