6-甲氧基-1-萘满酮合成路线 （共 219 条）
反应条件
NaBiO3; silica gel Hydrolysis; 0.133333 h; microwave irradiation, solid phase reaction;
参考文献
Mitra, Alok Kumar; De, Aparna; Karchaudhuri, Nilay
Journal of Chemical Research - Part S, 1999 , # 5 p. 320 - 321
反应条件
1: 90 percent / LAH / tetrahydrofuran / 5 h / Heating 2: 44 percent / red P, resublimed iodine / 5 h / 145 - 150 °C 3: 62 percent / BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) 3 h, 0 deg C; 2.) room temp., 2 h 4: 78 percent / DMTSF / CH2Cl2 / 0.25 h / Ambient temperature; effect of various Lewis acids on cyclization followed hydrolyzis View Scheme
参考文献
Tetrahedron, , vol. 43, # 8 p. 1847 - 1856
反应条件
1: 34 percent / MgCO3 / H2O; acetone / 22 h / Heating 2: aq. alkaline tetrahydrofuran / 22 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 28 p. 3007 - 3010
反应条件
1: 40 percent / MgCO3 / dioxane / 22 h / Heating 2: aq. alkaline tetrahydrofuran / 22 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 28 p. 3007 - 3010
反应条件
1: LiAlH4 / tetrahydrofuran 2: HBr 5: n-Bu4NF / hexamethylphosphoric acid triamide / 2 h / 40 °C 6: 1 M HCl / acetone / 1.5 h / Ambient temperature 7: 30 percent / 0.5 M Na2CO3, 0.5 M K3Fe(CN)6 / 3 h at 0 deg C, then 14 h at 25 deg C 8: diethyl ether View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4163 - 4164
反应条件
3: n-Bu4NF / hexamethylphosphoric acid triamide / 2 h / 40 °C 4: 1 M HCl / acetone / 1.5 h / Ambient temperature 5: 30 percent / 0.5 M Na2CO3, 0.5 M K3Fe(CN)6 / 3 h at 0 deg C, then 14 h at 25 deg C 6: diethyl ether View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4163 - 4164
反应条件
2: n-Bu4NF / hexamethylphosphoric acid triamide / 2 h / 40 °C 3: 1 M HCl / acetone / 1.5 h / Ambient temperature 4: 30 percent / 0.5 M Na2CO3, 0.5 M K3Fe(CN)6 / 3 h at 0 deg C, then 14 h at 25 deg C 5: diethyl ether View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4163 - 4164
反应条件
1: n-Bu4NF / hexamethylphosphoric acid triamide / 2 h / 40 °C 2: 1 M HCl / acetone / 1.5 h / Ambient temperature 3: 30 percent / 0.5 M Na2CO3, 0.5 M K3Fe(CN)6 / 3 h at 0 deg C, then 14 h at 25 deg C 4: diethyl ether View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4163 - 4164
反应条件
1: 1.) BuLi / 1.) hexane, THF, -78 deg C, 1 h, 2.) -78 deg C, 2 h 2: 1.) BuLi / 1.) hexane, THF, -10 deg C, 2 h, 2.) -10 deg C, 2.5 h 3: silver triflate / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
