1-[2-[4-(3-甲氧基-8-苯基-6,7,8,9-四氢-5H-苯并[7]轮烯-9-基)苯氧基]乙基]吡咯烷合成路线 （共 5 条）
反应条件
potassium carbonate in acetone 24 h; Heating;
参考文献
Sangwan, Naresh K.; Prasad, Mohan; Rastogi, Shri Nivas; Jehan, Qaiser; Setty, B. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 832 - 837
反应条件
1: 66 percent / PBr3 / benzene / 5 h / Ambient temperature 2: 1) NaH / 1.) DMF, 40-50 deg C, 30 min, 2.) DMF, r.t., 3 h 3: 68 percent / KOH / H2O; ethane-1,2-diol / 24 h / Heating 4: 65 percent / PPA / 0.5 h / 85 °C 5: 93 percent / KBH4 / methanol / 3 h / Ambient temperature 6: 40 percent / AlCl3 / benzene; hexane / 72 h / Ambient temperature 7: 80 percent / K2CO3 / acetone / 24 h / Heating View Scheme
参考文献
Sangwan, Naresh K.; Prasad, Mohan; Rastogi, Shri Nivas; Jehan, Qaiser; Setty, B. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 832 - 837
反应条件
1: 1) NaH / 1.) DMF, 40-50 deg C, 30 min, 2.) DMF, r.t., 3 h 2: 68 percent / KOH / H2O; ethane-1,2-diol / 24 h / Heating 3: 65 percent / PPA / 0.5 h / 85 °C 4: 93 percent / KBH4 / methanol / 3 h / Ambient temperature 5: 40 percent / AlCl3 / benzene; hexane / 72 h / Ambient temperature 6: 80 percent / K2CO3 / acetone / 24 h / Heating View Scheme
参考文献
Sangwan, Naresh K.; Prasad, Mohan; Rastogi, Shri Nivas; Jehan, Qaiser; Setty, B. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 832 - 837
反应条件
1: 68 percent / KOH / H2O; ethane-1,2-diol / 24 h / Heating 2: 65 percent / PPA / 0.5 h / 85 °C 3: 93 percent / KBH4 / methanol / 3 h / Ambient temperature 4: 40 percent / AlCl3 / benzene; hexane / 72 h / Ambient temperature 5: 80 percent / K2CO3 / acetone / 24 h / Heating View Scheme
参考文献
Sangwan, Naresh K.; Prasad, Mohan; Rastogi, Shri Nivas; Jehan, Qaiser; Setty, B. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 832 - 837
反应条件
1: 40 percent / AlCl3 / benzene; hexane / 72 h / Ambient temperature 2: 80 percent / K2CO3 / acetone / 24 h / Heating View Scheme
参考文献
Sangwan, Naresh K.; Prasad, Mohan; Rastogi, Shri Nivas; Jehan, Qaiser; Setty, B. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 832 - 837
