4,7-二氯喹啉 1-氧化物合成路线 (共 3 条)
反应条件
2-bromopyridine N-oxide; urea-hydrogen peroxide complex; potassium carbonate in 1,4-dioxane T=12 - 50°C; Baeyer-Villiger oxidation;
参考文献
Larionov, Oleg V.; Stephens, David; Mfuh, Adelphe M.; Arman, Hadi D.; Naumova, Anastasia S.; Chavez, Gabriel; Skenderi, Behije
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 19 p. 3026 - 3036
反应条件
copper(l) chloride; magnesium chloride in diethyl ether T=23°C; Grignard Reaction; 12 h; Inert atmosphere;
参考文献
Larionov, Oleg V.; Stephens, David; Mfuh, Adelphe; Chavez, Gabriel
Organic Letters, 2014 , vol. 16, # 3 p. 864 - 867
反应条件
trichlorophosphate
1.5 h; Heating / reflux;
参考文献
SCHERING AKTIENGESELLSCHAFT
Patent: WO2004/2960 A1, 2004 ;
Location in patent: Page 67-68 ;
WO 2004/002960 A1