反应条件
1: allyl bromide With chloro-trimethyl-silane; 1,1-dibromo ethane; zinc in tetrahydrofuran
T=25°C; 1 h;
2: (E)-(3-chloro-1-propenyl)benzene With N,N,N',N,-tetramethylethylenediamine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran
T=-20°C; 1.5 h; Title compound not separated from byproducts;
参考文献
Yasui, Hiroto; Mizutani, Keiya; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 7 p. 1410 - 1415