乙基丙酮酸酯-3-甲酰氨基-4-甲氧基苯基腙合成路线 （共 3 条）
反应条件
sodium acetate in ethanol; water T=-8°C; 22.2 h;
参考文献
Noar, J. Barry; Bruice, Thomas C.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1942 - 1945
反应条件
1: 69 percent / HCl / ethanol / 15 h / Ambient temperature 2: 5 percent / HCl / 1.) EtOH, 1 h, RT, 2.) reflux, 18 h 3: 95 percent / (NH4)2Ce(NO3)6 / H2O; acetonitrile / 0.33 h / 0 °C 4: 66 percent / 0.1M K2CO3 / 16 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 10 p. 1942 - 1945
参考文献
CLF MEDICAL TECHNOLOGY ACCELERATION PROGRAM, INC.
Patent: WO2006/102642 A1, 2006 ;
Location in patent: Page/Page column 9; 14; 1/6 ;
