2,6-二氨基-2',3'-二脱氧嘌呤-9-呋喃核糖苷合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated charcoal in methanol atmospheric pressure;
参考文献
Robins, Morris J.; Wilson, John S.; Madej, Danuta; Tyrrell, D. Lorne J.; Gati, Wendy P.; Lindmark; Wnuk, Stanislaw F.
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 6 p. 1297 - 1306
反应条件
2: 87 percent / H2 / 5percent Pd/C / ethanol / 20 h / 19 - 22 °C / 517.1 Torr View Scheme
参考文献
Robins, Morris J.; Wilson, John, S.; Madej, Danuta; Low, Nicholas H.; Hansske, Fritz; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7902 - 7908
反应条件
1: 90 percent / imidazole / dimethylformamide / 18 h / 20 °C 2: 96 percent / DMAP / acetonitrile / 1 h / 20 °C 3: 99 percent / (EtO)3P / 8 h / 100 - 115 °C 4: 81 percent / TBAF / tetrahydrofuran / 0.17 h / 0 °C 5: 47 percent / NH3 / methanol / 36 h / 90 °C 6: 99 percent / H2 / 10 percent Pd/C / methanol / atmospheric pressure View Scheme
参考文献
Robins, Morris J.; Wilson, John S.; Madej, Danuta; Tyrrell, D. Lorne J.; Gati, Wendy P.; Lindmark; Wnuk, Stanislaw F.
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 6 p. 1297 - 1306
