4-甲基苯甲酰甲醛水合物合成路线 （共 26 条）
反应条件
potassium cyanide in ethanol; water
参考文献
Peter, Matthias; Gleiter, Rolf; Rominger, Frank; Oeser, Thomas
European Journal of Organic Chemistry, 2004 , # 15 p. 3212 - 3220
参考文献
Veibel; Darling
Enzymol., 1939 , vol. 7, p. 348,349
Show Details
Veibel; Hansen
Enzymol., 1940 , vol. 9, p. 180
反应条件
acetic acid in 1,4-dioxane; water
参考文献
Nakamura, Akira; Ataka, Toshiei; Segawa, Hirozo; Takeuchi, Yasutomo; Takematsu, Tetsuo
Agricultural and Biological Chemistry, 1983 , vol. 47, # 7 p. 1555 - 1560
反应条件
in ethanol
3.5 h; Heating;
参考文献
Pokhariyal, G. P.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 401 - 402
反应条件
1: 80 percent / acetonoxime, 2 N HCl / H2O; methanol / 2 h / 50 °C / pH 4
2: 81 percent / methanol / 120 h
3: 96 percent / NH3(g) / propan-1-ol / 36 h / Ambient temperature
4: 89 percent / Na2S2O4 / H2O / 24 h / Heating
5: 32 percent / acetic anhydride / 2 h / Heating
6: 87 percent / xanthine oxidase (AXO) / 120 h / 4N NaOH, potassium phosphate buffer, pH 8.0
View Scheme
参考文献
Meester, Johan W. G. De; Plas, Henk C. van der; Middelhoven, Wouter J.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 441 - 451
反应条件
chloro-trimethyl-silane
18 h; Ambient temperature;
参考文献
Chan, T. H.; Brook, Michael A.; Chaly, T.
Synthesis, 1983 , # 3 p. 203 - 205
