4-苯基-1,3-二氧戊环合成路线 （共 7 条）
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=-78°C; 0.25 h; 2: With tri-n-butyl-tin hydride in dichloromethane 8 h;
参考文献
Xxx
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, # 7 p. 529 - 540
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; 2,6-di-tert-butyl-4-methyl-phenol in acetonitrile T=20°C; 0.5 h; Inert atmosphere;
参考文献
Maegawa, Tomohiro; Koutani, Yasuyuki; Otake, Kazuki; Fujioka, Hiromichi
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3384 - 3390
反应条件
manganese; sodium iodide; PbCl2 in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Hojo, Makoto; Aihara, Hidenori; Suginohara, Yoshifusa; Sakata, Kyosuke; Nakamura, Shin-ya
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8610 - 8611
反应条件
2,4-dichloro-6-methoxy-[1,3,5]triazine in toluene T=80°C; 4.5 h;
参考文献
Chu, Guobiao; Zhang, Yanqiao; Li, Chunbao; Zhang, Yuqing
Synthesis, 2009 , # 22 art. no. F12109SS, p. 3828 - 3832
参考文献
Verley
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1899 , vol. 128, p. 316
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 229
Chem. Zentralbl., 1900 , vol. 71, # II p. 359
Full Text Show Details
Verley
Patent: DE109176 ;
反应条件
bromine 1) 15 deg C, 20 min; 2) rt, 1 h; 3) 80 deg C, 21 h; further reagent: HBr; Product distributionMechanism;
参考文献
Krasnokutskaya; Habicher; Yusubov; Filimonov
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 2 p. 153 - 157
参考文献
Verley
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1899 , vol. 128, p. 316
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 229
Chem. Zentralbl., 1900 , vol. 71, # II p. 359
Full Text Show Details
Verley
Patent: DE109176 ;
