2,5-二溴-1,4-二甲基苯合成路线 (共 51 条)
反应条件
bromine in dichloromethane T=0 - 20°C; 24 h;
参考文献
Huang, Chibao; Qu, Junle; Qi, Jing; Yan, Meng; Xu, Gaixia
Organic Letters, 2011 , vol. 13, # 6 p. 1462 - 1465
反应条件
1: glacial acetic acid; bromine 2: hydrobromic acid 3: diluted hydrobromic acid / Diazotization.Verkochen der Diazonium-Loesung mit Kupferpulver und Kaliumbromid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 45, p. 2000
反应条件
bromine; nitrogen(IV) oxide in water; trifluoroacetic acid T=20°C; 0.1 h; other time; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, # 2 p. 217 - 223
Zhurnal Organicheskoi Khimii, , vol. 24, # 2 p. 248 - 255
参考文献
Henichart, J. P.; Bernier J. L.; Vaccher, C.; Houssin, R.; Warin, V.; Baert, F.
Tetrahedron, 1980 , vol. 36, p. 3535 - 3542
反应条件
aluminum oxide; bromine 0.0166667 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 22, # 8 p. 1095 - 1099
参考文献
Chemische Berichte, , vol. 10, p. 1355
参考文献
Chemische Berichte, , vol. 18, p. 357
反应条件
1: sodium hydroxide; potassium permanganate / H2O / 12 h / Heating 2: SOCl2 / 4 h / Heating 3: 2.1 g / 4 h / Heating View Scheme
参考文献
Cai, Liping; Moehl, Thomas; Moon, Soo-Jin; Decoppet, Jean-David; Humphry-Baker, Robin; Xue, Zhaosheng; Bin, Liu; Zakeeruddin, Shaik M; Graetzel, Michael
Organic Letters, 2014 , vol. 16, # 1 p. 106 - 109
反应条件
1: KMnO4; pyridine 2: H2SO4 View Scheme
参考文献
Pham, Van Chung; Huh, Geun; Kim, Jungahn; Choo, Dong Joon; Lee, Jae Yeol
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1781 - 1783