N3-甲基-5-苯基-2,3-吡啶二胺合成路线 （共 10 条）
反应条件
copper(II) sulfate in water T=200°C; 72 h; Heating;
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
in trifluoroacetic acid 2 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: pyridine / Heating 2: K2CO3 / acetone / Ambient temperature 3: 68 percent / I2 / H2O; acetic acid / 80 °C 4: 45 percent / trifluoroacetic acid / 2 h / Irradiation View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: K2CO3 / acetone / Ambient temperature 2: 68 percent / I2 / H2O; acetic acid / 80 °C 3: 45 percent / trifluoroacetic acid / 2 h / Irradiation View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: 68 percent / I2 / H2O; acetic acid / 80 °C 2: 45 percent / trifluoroacetic acid / 2 h / Irradiation View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: 58 percent / NaNH2 / toluene 2: 3.1 g / Br2 / acetic acid / 1 h / Ambient temperature 3: CuSO4 / H2O / 72 h / 200 °C / Heating View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
1: 3.1 g / Br2 / acetic acid / 1 h / Ambient temperature 2: CuSO4 / H2O / 72 h / 200 °C / Heating View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
in ethanol T=175°C; 1 h; Yield given;
参考文献
Knize, Mark G.; Felton, James S.
Heterocycles, 1986 , vol. 24, # 7 p. 1815 - 1819
反应条件
1: Heating 2: 80 percent / NaNH2 View Scheme
参考文献
Bavetta, Fabio S.; Caronna, Tullio; Pregnolato, Massimo; Terreni, Marco
Tetrahedron Letters, 1997 , vol. 38, # 44 p. 7793 - 7796
反应条件
Heating; Yield given;
参考文献
Bavetta, Fabio S.; Caronna, Tullio; Pregnolato, Massimo; Terreni, Marco
Tetrahedron Letters, 1997 , vol. 38, # 44 p. 7793 - 7796
