3-(疏基甲基)-1-阿杂环[2.2.2]辛烷-3-醇合成路线 （共 9 条）
反应条件
hydrogen sulfide in methanol; dichloromethane T=0 - 5°C;
参考文献
Pramanik, Chinmoy; Patil, Pradip; Kotharkar, Sandeep; Tripathy, Narendra K.; Gurjar, Mukund K.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3043 - 3045
反应条件
hydrogen sulfide; sodium hydroxide in water T=45°C; 2.5 h;
参考文献
Pramanik, Chinmoy; Patil, Pradip; Kotharkar, Sandeep; Tripathy, Narendra K.; Gurjar, Mukund K.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3043 - 3045
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US5571918 A1, 1996 ;
反应条件
1.1: potassium tert-butylate / dimethyl sulfoxide / 0.5 h / 25 - 30 °C / |Inert atmosphere 1.2: 8 h / 25 °C / |Inert atmosphere 2.1: hydrogen sulfide; sodium hydroxide / water / 2.5 h / 45 °C View Scheme
参考文献
Pramanik, Chinmoy; Patil, Pradip; Kotharkar, Sandeep; Tripathy, Narendra K.; Gurjar, Mukund K.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3043 - 3045
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US5571918 A1, 1996 ;
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane 2: With hydrogenchloride in diethyl ether
参考文献
Pramanik, Chinmoy; Patil, Pradip; Kotharkar, Sandeep; Tripathy, Narendra K.; Gurjar, Mukund K.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3043 - 3045
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=0 - 25°C; 2: With sodium hydroxide in dichloromethane; water pH=12 - 14;
参考文献
APICORE, LLC
Patent: US2011/301352 A1, 2011 ;
Location in patent: Page/Page column 3 ;
反应条件
sodium hydroxide; sulfuric acid; sodium sulfate in chloroform
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US5571918 A1, 1996 ;
反应条件
sodium hydroxide; sulfuric acid in chloroform
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US5571918 A1, 1996 ;
