5-甲基-1,3-恶唑烷-2-酮合成路线 （共 21 条）
反应条件
sodium hydride in tetrahydrofuran
18 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Motherwell, William B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1124 - 1131
反应条件
hydrogenchloride in methanol
1) 15 min, 0 deg C; 2) 15 min, room temp.;
参考文献
Miyahara; Nakadate; Kamiya
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 2 p. 497 - 502
反应条件
in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Kim, Sunggak; Ko, Young Kwan
Heterocycles, 1986 , vol. 24, # 6 p. 1625 - 1630
反应条件
hydrogenchloride in tetrahydrofuran; N,N-dimethyl-formamide
T=65°C;
参考文献
Hu, Qiao-Sheng; Sheng, Shou-Ri; Lin, Shu-Ying; Wei, Mei-Hong; Xin, Qin; Liu, Xiao-Ling
Journal of Chemical Research, 2007 , # 2 p. 74 - 75
反应条件
T=180°C; P=75007.5 Torr; 24 h; Autoclave;
参考文献
Wu, Chaoyong; Cheng, Haiyang; Liu, Ruixia; Wang, Qiang; Hao, Yufen; Yu, Yancun; Zhao, Fengyu
Green Chemistry, 2010 , vol. 12, # 10 p. 1811 - 1816
反应条件
methanol; sulfur
T=120°C;
参考文献
Monsanto Chem. Co.
Patent: US2857392 , 1956 ;
反应条件
P=165017 Torr; 24 h;
参考文献
Ihata, Osamu; Kayaki, Yoshihito; Ikariya, Takao
Macromolecules, 2005 , vol. 38, # 15 p. 6429 - 6434
参考文献
Kricheldorf,H.R.
Chemische Berichte, 1970 , vol. 103, p. 3353 - 3355
反应条件
in N,N-dimethyl-formamide
参考文献
Barton, Derek H. R.; Motherwell, William B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1124 - 1131
反应条件
(i) aq. KOH, (ii) /BRN= 385737/, MeOH; Multistep reaction;
参考文献
Newman,M.S.; Din,Z.U.
Journal of Organic Chemistry, 1973 , vol. 38, p. 547 - 549
