2,2,5,5-四甲基己烷合成路线 （共 25 条）
反应条件
tetra-n-butylammonium perchlorate; nickel(II) chlorate(VII); triphenylphosphine in acetonitrile
T=25°C;
参考文献
Schiavon, Gilberto; Bontempelli, Gino; Corain, Benedetto
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1074 - 1081
反应条件
lithium in diethyl ether
Heating;
参考文献
Pine,S.H. et al.
Journal of Organic Chemistry, 1970 , vol. 35, # 11 p. 3663 - 3666
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 125
反应条件
sodium naphthalenide
参考文献
Sargent,G.D.; Lux,G.A.
Journal of the American Chemical Society, 1968 , vol. 90, p. 7160 - 7162
反应条件
tetrakislt;iodo(tri-n-butylphosphine)gt;copper(I); oxygen
Multistep reaction;
参考文献
Gorman, Christopher B.; Ginsburg, Eric J.; Grubbs, Robert H.
Journal of the American Chemical Society, 1993 , vol. 115, # 4 p. 1397 - 1409
参考文献
Howard et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2121
Journal of Research of the National Bureau of Standards (United States), vol. 38, p. 387,391
Chem.Abstr., 1947 , p. 5291
反应条件
in cyclohexane
(N2 or Ar); a mixture of Pt-complex and P(C2H5)3 in cyclohexane heated at 157°C for 1.6-2.25 h; cooled to -196°C; warmed to 25°C; evapd.; dissolved in acetonitrile; separated; evapd.; dissolved in ether; methanol added; cooled to -78°C; concentrated; pptd.; recrystd. from methanol/ether; elem. anal.;
参考文献
Foley, Paul; DiCosimo, Robert; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 22 p. 6713 - 6725
反应条件
hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane
T=25°C; Thermodynamic dataRate constant;
参考文献
Doering, William v. E.; Roth, Wolfgang R.; Bauer, Frank; Breuckmann, Rolf; Ebbrecht, Thomas; at al.
Chemische Berichte, 1989 , vol. 122, p. 1263 - 1276
反应条件
hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane
T=25°C; Thermodynamic dataRate constant;
参考文献
Doering, William v. E.; Roth, Wolfgang R.; Bauer, Frank; Breuckmann, Rolf; Ebbrecht, Thomas; at al.
Chemische Berichte, 1989 , vol. 122, p. 1263 - 1276
反应条件
hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane
T=25°C; ΔHH; Thermodynamic data;
参考文献
Roth, Wolfgang R.; Hopf, Henning; Horn, Carina
Chemische Berichte, 1994 , vol. 127, # 9 p. 1781 - 1796
