6-氯-6-氧代己酸乙酯合成路线 （共 76 条）
反应条件
thionyl chloride 1.5 h; Heating;
参考文献
Regourd, Jasmine; Ali, Adeeb Al-Sheikh; Thompson, Alison
Journal of Medicinal Chemistry, 2007 , vol. 50, # 7 p. 1528 - 1536
参考文献
Sakuragi; Tokumaru; Itoh; Terakawa; Kikuchi; Caldwell; Hsu
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1049 - 1057
反应条件
1: 83 percent / tetrafluorophthalic anhydride / 60 h / 135 °C 2: thionyl chloride / Heating View Scheme
参考文献
Eaton, Jefferson T.; Rounds, William D.; Urbanowicz, John H.; Gribble, Gordon W.
Tetrahedron Letters, 1988 , vol. 29, # 50 p. 6553 - 6556
反应条件
1: H2SO4 2: SOCl2 View Scheme
参考文献
Blaise; Koehler
Bulletin de la Societe Chimique de France, 1910 , vol. <4>7, p. 219
反应条件
lithium tetrachloromanganate(II) in tetrahydrofuran T=0 - 10°C; 0.5 h;
参考文献
Cahiez, Gerard
Tetrahedron Letters, 1992 , vol. 33, # 31 p. 4439 - 4442
参考文献
Cason,J.; Schmitz,F.J.
Journal of Organic Chemistry, 1963 , vol. 28, p. 552 - 555
参考文献
Yoshioka
Yakugaku Zasshi, 1955 , vol. 75, p. 606
Chem.Abstr., 1956 , p. 795
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Moroe
Yakugaku Zasshi, 1950 , vol. 70, p. 416,422
Yakugaku Zasshi, 1951 , vol. 71, p. 123
反应条件
1: 76 percent / tin(IV) chloride / CH2Cl2 / 1.5 h / Ambient temperature 2: 91 percent / 95percent hydrazine hydrate, potassium hydroxide / ethane-1,2-diol / 4.5 h / 60 °C / Heating 3: 85 percent / Raney nickel-aluminium alloy / aq. NaOH / 3 h / 90 - 120 °C View Scheme
参考文献
Jefferson, Alan; Sargent, Melvyn V.; Wangchareontrakul, Sirichai
Australian Journal of Chemistry, 1988 , vol. 41, # 1 p. 19 - 25
反应条件
aluminium trichloride Behandeln des Reaktionsprodukts mit aethanol. Natronlauge;
参考文献
Christol,H.; Plenat,F.
Bulletin de la Societe Chimique de France, 1962 , p. 1325 - 1331
反应条件
benzene Erhitzen des Reaktionsprodukts mit wss.-aethanol. Natronlauge;
参考文献
Kornblum; Iffland
Journal of the American Chemical Society, 1949 , vol. 71, p. 2137,2138,2140
