三甲基-三甲基锡烷基硫基锡烷合成路线 （共 16 条）
反应条件
methyl iodide in pentane Sn sulfide and MeI refluxing in pentane for 25 h, sulfonium salt filtering off; Sn containing products analyzed by GLC;
参考文献
Razuvaev, G.A.; Shcherbakov, V.I.; Grigor'Eva, I.K.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 245 - 252
反应条件
in [3.3.1]nonane Sn sulfide and freshly pptd. Cu heating in nonane in a sealed tube for 40 h at 160°C, liquid fraction decanting off, solid washing with nonane, solvent removing from combined solns.; Me2SnO isolated as Me2SnCl2;
参考文献
Razuvaev, G.A.; Shcherbakov, V.I.; Grigor'Eva, I.K.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 245 - 252
反应条件
in [3.3.1]nonane Sn sulfide and freshly pptd. Cu heating in nonane in a sealed tube for 40 h at 160°C, liquid fraction decanting off, solid washing with nonane, solvent removing from combined solns.; Me2SnO isolated as Me2SnCl2;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 245 - 252
反应条件
in neat (no solvent)
Irradiation (UV/VIS); Sn-compd. placed in sealed flask, exposed to daylight radiation for 48 h; solid dissolved in cyclohexane, recrystd., washed; identified by m.p., elem. anal., IR and mass spectra;
参考文献
Craig, Peter J.; Rapsomanikis, Spyridon
Journal of the Chemical Society, Chemical Communications, 1982 , p. 114
反应条件
sodium in neat (no solvent)
addn. of Na to soln. of Sn compound in aromatic hydrocarbon (N2 atmosphere), reflux; fractional distn.;
参考文献
Capozzi, Giuseppe; Menichetti, Stefano; Ricci, Alfredo; Taddei, Maurizio
Gazzetta Chimica Italiana, 1990 , vol. 120, # 11 p. 721 - 722
反应条件
sodium in tetrahydrofuran
addn. of Na to soln. of Sn compound and sulphide (N2 atmosphere), reflux (0.6 h),; cooling, addn. n-pentane, filtration, TLC (light petroleum);
参考文献
Capozzi, Giuseppe; Menichetti, Stefano; Ricci, Alfredo; Taddei, Maurizio
Gazzetta Chimica Italiana, 1990 , vol. 120, # 11 p. 721 - 722
