反应条件
in pentane byproducts: LiCl; inert atmosphere, addn. of soln. of (CH3)3SnCl to suspension of Li2C2 at-25°C (40 min), warming to room temp., reflux (1 h); filtration from LiCl, concn., recrystn. (pentane, -78°C), drying (40°C, 5 Torr);
参考文献
Eisch, John J.; Kotowicz, Boguslaw W.
European Journal of Inorganic Chemistry, 1998 , # 6 p. 761 - 769
