N-重氮基氨基甲酸叔-丁基酯合成路线 （共 237 条）
反应条件
TEA in 1,4-dioxane; water 24 h; Ambient temperature;
参考文献
Huffman; Gesellchen; Turner; Rothenberger; Osborne; Miller; Chapman; Queener
Journal of Medicinal Chemistry, 1992 , vol. 35, # 10 p. 1897 - 1914
反应条件
1: pyrrole With potassium T=22°C; Inert atmosphere; 2: tert-butyloxycarbonyl azide in tetrahydrofuran T=0°C; 5 h; Inert atmosphere;
参考文献
Koh, Ming Joo; Khan, R. Kashif M.; Torker, Sebastian; Hoveyda, Amir H.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 7 p. 1968 - 1972
Angew. Chem., 2014 , vol. 126, # 7 p. 1999 - 2003,5
参考文献
Khan,S.A.; Sivanandaiah,K.M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15, p. 80 - 81
反应条件
1: Et3N / methanol 2: aq. HCl, AcOH View Scheme
参考文献
Fuchs,S.; Voelter,W.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1976 , vol. 31, p. 1410 - 1415
反应条件
magnesium oxide in 1,4-dioxane; water
参考文献
Arold,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 490 - 496
参考文献
Hofmann,K. et al.
Journal of the American Chemical Society, 1965 , vol. 87, p. 611 - 619
参考文献
Khan,S.A.; Sivanandaiah,K.M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15, p. 80 - 81
反应条件
1: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge 2: aq. NaOH solution View Scheme
参考文献
Carpino et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 955
参考文献
Carpino et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 955
反应条件
1: 97 percent / 2 N aq. NaOH / dioxane / 4 h / 50 °C View Scheme
参考文献
Lipkowski, Andrzej W.; Flouret, George
Polish Journal of Chemistry, 1980 , vol. 54, # 11/12 p. 2225 - 2228
