N-重氮基氨基甲酸叔-丁基酯合成路线 （共 237 条）
反应条件
potassium hydrogencarbonate; sodium nitrite in water; acetic acid
参考文献
Synthelabo
Patent: US4134991 A1, 1979 ;
反应条件
sodium azide; 18-crown-6 ether in tetrahydrofuran T=20°C; 96 h;
参考文献
Holzinger, Michael; Abraham, Juergen; Whelan, Paul; Graupner, Ralf; Ley, Lothar; Hennrich, Frank; Kappes, Manfred; Hirsch, Andreas
Journal of the American Chemical Society, 2003 , vol. 125, # 28 p. 8566 - 8580
参考文献
Merck and Co., Inc.
Patent: US4558071 A1, 1985 ;
反应条件
(i) Py, Et2O, (ii) N,N,N',N'-tetramethyl-guanidine azide, CHCl3; Multistep reaction;
参考文献
Sakai,K.; Anselme,J.-P.
Journal of Organic Chemistry, 1971 , vol. 36, # 16 p. 2387 - 2388
反应条件
1: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge View Scheme
参考文献
Carpino et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 955
反应条件
anhydrous magnesium hydroxide in 1,4-dioxane; water T=40°C; 20 h;
参考文献
Lee, Heejoo; Fong, Kei-Lai; Vince, Robert
Journal of Medicinal Chemistry, 1981 , vol. 24, # 3 p. 304 - 308
反应条件
(i) MgCO3, aq. dioxane, (ii) /BRN= 1363586/; Multistep reaction;
参考文献
Anderson; Barton; Hardy; Kenner; Preston; Sheppard
Journal of the Chemical Society. Perkin transactions 1, 1967 , vol. 1, p. 108 - 113
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 12 p. 1361 - 1363
反应条件
sodium hydroxide in tetrahydrofuran; water 2 h; Ambient temperature; Yield given;
参考文献
Anjaneyulu B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 657 - 661
反应条件
magnesium oxide in 1,4-dioxane; water
参考文献
Bentley,P.H. et al.
Journal of the Chemical Society, 1964 , p. 6130 - 6138
