2-甲基-2,4-戊二醇合成路线 (共 135 条)
反应条件
nickel Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 62, p. 2448
Journal of the American Chemical Society, , vol. 52, p. 4349,4354
反应条件
hydrogen; palladium hydroxide - carbon in ethanol P=760 Torr;
参考文献
Poss, A. J.; Smyth, M. S.
Synthetic Communications, 1989 , vol. 19, # 19 p. 3363 - 3366
反应条件
hydrogen fluoride in acetonitrile T=25°C; 0.25 h;
参考文献
Corey, E. J.; Hopkins, Paul B.
Tetrahedron Letters, 1982 , vol. 23, # 47 p. 4871 - 4874
反应条件
hydrogen fluoride in acetonitrile T=25°C; 12 h;
参考文献
Corey, E. J.; Hopkins, Paul B.
Tetrahedron Letters, 1982 , vol. 23, # 47 p. 4871 - 4874
反应条件
(i-PrS)BBr in dichloromethane T=-78°C;
参考文献
Corey, E. J.; Hua, Duy H.; Seitz, Steven P.
Tetrahedron Letters, 1984 , vol. 25, # 1 p. 3 - 6
反应条件
potassium carbonate in methanol T=23°C;
参考文献
Chen, Ke; Richter, Jeremy M.; Baran, Phil S.
Journal of the American Chemical Society, 2008 , vol. 130, # 23 p. 7247 - 7249
反应条件
lithium perchlorate; phenyl-hydroxy-acetic acid T=20°C; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 8 p. 1361 - 1363
反应条件
lithium perchlorate; phenyl-hydroxy-acetic acid T=20°C; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 8 p. 1361 - 1363
反应条件
1: With tin(IV) chloride in nitromethane T=-10 - 20°C; Addition; Salt formation; 1 h; 2: With water Hydrolysis; 3: With potassium hydroxide in ethanol Hydrolysis; 0.75 h; Heating;
参考文献
Russian Journal of Organic Chemistry, , vol. 35, # 11 p. 1593 - 1599
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane T=20°C;
参考文献
Nedogrel, E. P.; Musavirov, R. S.; Zhurkina, I. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 937 - 940,856 - 859