反应条件
in toluene
dropwise addn. of soln. of Fe(CO)5 to soln. of amine, -78°C, warming up to room temp., evapn., addn. of pentane, pptn. of Me3SnNCO, filtration, evapn. in vac., under N2; extn. with pentane, chromy. (Al2O3), evapn. in vac., elem. anal. of Me3SnNCO;
参考文献
Petz, Wolfgang; Wrackmeyer, Bernd; Storch, Wolfgang
Chemische Berichte, 1989 , vol. 122, p. 2261 - 2264
