in methanol
Sn-complex and ligand were stirred in MeOH at room temp. for ca. 12 h; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;
参考文献
Cunningham, Desmond; Firtear, Padraig; Molloy, Kiaran C.; Zuckerman, Jerald J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1523 - 1528
in acetone
soln. of ligand in acetone was added with stirring to soln. of Sn-complex in acetone, stirred for several h at room temp.; filtered, washed with EtOH, dried under vac. at 20°C for 10 h;
参考文献
Cunningham, Desmond; Firtear, Padraig; Molloy, Kiaran C.; Zuckerman, Jerald J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1523 - 1528
