Nash, G. A.; Skinner, H. A.; Stack, W. F.
Transactions of the Faraday Society, 1965 , vol. 61, p. 640 - 648
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
POCl3, P2O5 8.887 g (C2H5)2SnCl2, 65.7 ml POCl3, and 12.78 g P2O5 added to 23.49 g SnCl4 added at 0°C with stirring; heated at 130°C for 48 h;diluted with benzene; filtered; C6H6 and POCl3 evaporated under atm. pr essure; vacuum-distilled;
参考文献
Mingalev; Rzhevskii; Perfil'ev; Lisichkin
Russian Journal of Applied Chemistry, 2000 , vol. 73, # 6 p. 947 - 951
