1: 3-oxo-butyric acid isobutyl ester With sodium hydride in tetrahydrofuran 2: With n-butyllithium 3: chloromethyl benzyl ether
参考文献
Kim, Yong-Jae; Wang, Pengfei; Navarro-Villalobos, Mauricio; Ronde, Bridget D.; Derryberry, JohnMark; Gin, David Y.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11906 - 11915
1: 3-oxo-butyric acid isobutyl ester With sodium hydride in tetrahydrofuran T=0°C; 0.75 h; 2: With n-butyllithium in tetrahydrofuran; hexane T=-25°C; 0.75 h; 3: benzyl chloroformate in tetrahydrofuran; hexane T=-25°C; 1 h;
参考文献
Blakemore, Paul R.; Browder, Cindy C.; Hong, Jian; Lincoln, Christopher M.; Nagornyy, Pavel A.; Robarge, Lonnie A.; Wardrop, Duncan J.; White, James D.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5449 - 5460