1-溴-2-溴甲基-3-羟基丙烷合成路线 (共 4 条)
反应条件
diborane in dichloromethane 1.) 0 deg C, 1 h; 2.) room temp., overnight;
参考文献
Symbicom Aktiebolag
Patent: US4868289 A1, 1989 ;
反应条件
pyridine; acetic anhydride in ethyl acetate
参考文献
SYMBICOM AB
Patent: EP210203 B1, 1991 ;
反应条件
in pyridine 17 h; Ambient temperature;
参考文献
Ansari, Akbar A.; Frejd, Torbjoern; Magnusson, Goeran
Carbohydrate Research, 1987 , vol. 161, p. 225 - 234
反应条件
boron trifluoride diethyl etherate in dichloromethane 24 h; Ambient temperatureother solvebt, reaction time; Product distribution;
参考文献
Ellervik, Ulf; Jansson, Karl; Magnusson, Goeran
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 4-5 p. 777 - 784