1,1,3,3-四乙氧基-2-甲基丙烷合成路线 （共 23 条）
反应条件
water; toluene-4-sulfonic acid
参考文献
Klimko,V.T. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, p. 2961 - 2966,2913 - 2918
反应条件
hydrogenchloride; potassium hydroxide 1) 80 deg C, 1 h; Multistep reaction;
参考文献
Ullrich, Friedrich-Wilhelm; Rotscheidt, Klaus; Breitmaier, Eberhard
Chemische Berichte, 1986 , vol. 119, # 5 p. 1737 - 1744
反应条件
hydrogenchloride in water T=95°C; sealed tube;
参考文献
US2012/15962 A1, ;
Page/Page column 90 ;
US 20120015962 A1
反应条件
1: With monohydrazine sulfate in water T=80°C; 3 h; 2: With sodium hydroxide in water T=3 - 30°C; pH=4 - 6; 3: With sodium hydrogencarbonate in water T=27 - 30°C; pH=7;
参考文献
Reardan, Dayton T.; Combe, Michel D.
Patent: US2007/244330 A1, 2007 ;
Location in patent: Page/Page column 2; 3 ;
反应条件
hydroxylamine hydrochloride
参考文献
Wilson,B.D.; Burness,D.M.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1565 - 1569
反应条件
zinc(II) chloride in acetic anhydride
参考文献
Shramova,Z.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1966 , vol. 2, p. 1005 - 1009
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1014 - 1019
反应条件
in water T=70°C; 3 h;
参考文献
Zaitsev; Dalinger; Starosotnikov; Kachala; Strelenko; Shkineva; Shevelev
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 10 p. 1507 - 1515
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 14 h;
参考文献
Mamat, Constantin; Buettner, Stefan; Trabhardt, Tiana; Fischer, Christine; Langer, Peter
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6273 - 6275
反应条件
sulfuric acid in ethanol; water 3 h; Heating;
参考文献
Pavlik, James W.; Connors, Robert E.; Burns, Douglas S.; Kurzweil, Edyth M.
Journal of the American Chemical Society, 1993 , vol. 115, # 17 p. 7645 - 7652
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 14 h;
参考文献
Mamat, Constantin; Buettner, Stefan; Trabhardt, Tiana; Fischer, Christine; Langer, Peter
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6273 - 6275
