1: With diethylaluminium chloride in dichloromethane T=-78°C; chelation; 0.5 h; 2: With tri-n-butyl-tin hydride T=-78°C; Reduction; 1 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 122, # 19 p. 4817 - 4818
1: With silver fluoride in acetonitrile T=20°C; 3 h; DarknessInert atmosphere; 2: With hydrogenchloride; water in acetonitrile T=20°C; 0.0833333 h; Inert atmosphere; chemoselective reaction;