2-(4-溴苯基)-1,3-二氧戊环合成路线 （共 37 条）
反应条件
toluene-4-sulfonic acid in toluene Reflux;
参考文献
Nishi, Hiroyasu; Namari, Tomoko; Kobatake, Seiya
Journal of Materials Chemistry, 2011 , vol. 21, # 43 p. 17249 - 17258
反应条件
p-toluenesulfonic acid monohydrate in ethylene glycol; benzene
参考文献
Bayer Corporation
Patent: US6355803 B1, 2002 ;
反应条件
toluene-4-sulfonic acid in hexane; ethyl acetate; benzene
参考文献
G. D. Searle and Co.
Patent: US4988707 A1, 1991 ;
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=-30°C; 1.5 h;
参考文献
Barbasiewicz, Michal; Makosza, Mieczyslaw
Organic Letters, 2006 , vol. 8, # 17 p. 3745 - 3748
反应条件
poly[4-(diacetoxyiodo)styrene]; iodine in acetonitrile T=30°C; 1 h; Irradiation;
参考文献
Teduka, Tomomasa; Togo, Hideo
Synlett, 2005 , # 6 art. no. U02605ST, p. 923 - 926
反应条件
toluene-4-sulfonic acid in toluene 48 h; Reflux;
参考文献
Mei; Wang; Qin; Zhao; Yuan; Sung; Deng; Zhang; Williams; Sun; Tang
Journal of Materials Chemistry, 2012 , vol. 22, # 10 p. 4290 - 4298
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.67 h / -78 °C 1.2: 77 percent / tetrahydrofuran / -78 - 20 °C 2.1: 75 percent / p-TsOH / tetrahydrofuran; H2O / 7 h / Heating View Scheme
参考文献
Hon, Yung-Son; Lee, Chia-Fu; Chen, Rong-Jiunn; Szu, Ping-Hui
Tetrahedron, 2001 , vol. 57, # 28 p. 5991 - 6001
反应条件
copper; sodium hydride 1.) DMF, RT, 2.) DMF, 150 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Cozzi, Paolo; Carganico, Germano; Fusar, Domenico; Grossoni, Mauro; Menichincheri, Maria; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 20 p. 2964 - 2972
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.67 h / -78 °C 1.2: 77 percent / tetrahydrofuran / -78 - 20 °C 2.1: 75 percent / p-TsOH / tetrahydrofuran; H2O / 7 h / Heating 3.1: 96 percent / tetrahydrofuran / 5 h / -78 - 20 °C View Scheme
参考文献
Hon, Yung-Son; Lee, Chia-Fu; Chen, Rong-Jiunn; Szu, Ping-Hui
Tetrahedron, 2001 , vol. 57, # 28 p. 5991 - 6001
