2-(三甲基硅基)乙烷磺酰氯合成路线 （共 11 条）
反应条件
thionyl chloride; N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Tetrahedron, , vol. 59, # 51 p. 10165 - 10171
反应条件
sulfuryl dichloride; triphenylphosphine in dichloromethane 1 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 33, # 19 p. 2657 - 2660
反应条件
phosphorus pentachloride in tetrachloromethane Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 27, # 19 p. 2099 - 2102
反应条件
1: 70 percent / NaHSO3, PhCO3t-Bu / methanol; H2O / 48 h / Heating 2: 60 percent / PCl5 / CCl4 / 1.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 19 p. 2099 - 2102
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: Cs2CO3 / dimethylformamide / 24 h / 20 °C
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: 76 percent / Cs2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: 73 percent / Cs2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: Cs2CO3 / dimethylformamide / 24 h / 20 °C
3: 96 percent / BH3*THF / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: 76 percent / Cs2CO3 / dimethylformamide / 20 °C
3: 95 percent / BH3*THF / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
反应条件
1: 88 percent / ammonia / CH2Cl2 / 2 h / 0 °C
2: 73 percent / Cs2CO3 / dimethylformamide / 20 °C
3: 97 percent / BH3*THF / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Parker, Laurie L.; Gowans, Nicholas D.; Jones, Stephen W.; Robins, David J.
Tetrahedron, 2003 , vol. 59, # 51 p. 10165 - 10171
