1,2-环氧-4-乙烯基环己烷合成路线 (共 24 条)
反应条件
tert.-butylhydroperoxide T=79.84°C; Green chemistry; Reagent/catalystTemperature;
参考文献
Mohammed, Misbahu Ladan; Patel, Dipesh; Mbeleck, Rene; Niyogi, Debdarsan; Sherrington, David C.; Saha, Basudeb
Applied Catalysis A: General, 2013 , vol. 466, p. 142 - 152
反应条件
dihydrogen peroxide; magnesium sulfate; methyltrioxorhenium (VII) in tert-butyl alcohol T=15°C; 2 h;
参考文献
Angewandte Chemie, , vol. 103, # 12 p. 1706 - 1709
反应条件
dihydrogen peroxide; TBA-[γ-SiW10O34(H2O)2]4- in acetonitrile T=31.85°C; 4 h; Product distribution; Further Variations:CatalystsReagents;
参考文献
Journal of Catalysis, , vol. 224, # 1 p. 224 - 228
反应条件
tert.-butylhydroperoxide; silica gel; β-MoO3 in decane T=50°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 10 p. 1123 - 1124
反应条件
[bis(acetoxy)iodo]benzene; 2BF4(1-)*C30H32N8O3Ru(2+) in dichloromethane T=20°C; 24 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Inorganic Chemistry, , vol. 50, # 13 p. 6044 - 6054
反应条件
disodium hydrogenphosphate; dihydrogen peroxide in chloroform 24 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 22, p. 2089 - 2092
反应条件
[.pi.-C5H5N(+)(CH2)15CH3]3(PMo12O40)(3-); dihydrogen peroxide; magnesium sulfate in chloroform T=60°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 14, # 9 p. 865 - 874
反应条件
dimethyllt;dioctadecyl(76percent) + dihexadecyl(24percent)gt;ammonium tetrakis(diperoxotungsto)phosphate; dihydrogen peroxide in benzene T=60°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 7 p. 1553 - 1557
反应条件
dihydrogen peroxide in water T=65°C; 1.5 h;
参考文献
Physical Chemistry Chemical Physics, , vol. 13, # 36 p. 16282 - 16294
反应条件
dihydrogen peroxide in water T=64.84°C; 2 h; regioselective reaction;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 328, # 1-2 p. 60 - 67