反应条件
1: 93 percent / H2 / Pd/C / methanol / 50 h / 20 °C 2: PCC / CH2Cl2 / 2 h / 20 °C 3: 82 percent / diethyl ether / 15 h / 20 °C 4: 1.) O3, O2, 2.) Me2S, 3.) Na2SO4, TsOH*H2O / 1.) CH2Cl2, MeOH, -65 deg C, 2.) -60 deg C, 1h; -15 deg C, 1 h; 0 deg C, 1 h; 20 deg C, 12 h, 3.) benzene, reflux, 1 h 5: 2.) 10percent H2SO4 / 1.) ether, -10 deg C, 3 h, 2.) 1h View Scheme
参考文献
Odinokov, V. N.; Ishmuratov, G. Yu.; Kharisov, R. Ya.; Serebryakov, E. P.; Tolstikov, G. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 1 p. 100 - 101
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 1 p. 110 - 112
