pyridine; PPh3.Br2 in tetrachloromethane; dichloromethane 3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: With sodium hydroxide; Na2MoO4 in methanol; water pH=11.7; 2: With dihydrogen peroxide in methanol; water T=55 - 73°C; 0.0833333 - 6 h; Conversion of starting material;
参考文献
Bourne, Richard A.; Han, Xue; Poliakoff, Martyn; George, Michael W.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 29 p. 5322 - 5325
Angewandte Chemie, 2009 , vol. 121, # 29 p. 5426 - 5429
triphenyl phosphite; ozone 1.) CH2Cl2, -80 deg C, 30 min; 2.) CH2Cl2, -80 deg C to room temp. then 2 h at room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wahlen, Joos; De Vos, Dirk; Jary, Walther; Alsters, Paul; Jacobs, Pierre
Chemical Communications, 2007 , # 23 p. 2333 - 2335
Khosropour, Ahmad R.; Khodaei, Mohammad M.; Ghaderi, Sattar
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 3 p. 326 - 330
