(二氯亚甲基)二磷酸四异丙酯合成路线 （共 7 条）
反应条件
sodium hypochlorite 0.333333 h; Ambient temperature;
参考文献
McKenna, Charles E.; Khawli, Leslie A.; Ahmad, Wan-Yaacob; Pham, Phuong; Bongartz, Jean-Pierre
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 37, p. 1 - 12
反应条件
2: aq. NaOCl, NaCl View Scheme
参考文献
Quimby,O.T. et al.
Journal of Organometallic Chemistry, 1968 , vol. 13, p. 199 - 207
反应条件
formic acid; tert-butylhypochlorite 2 h; Heating;
参考文献
McKenna, Charles E.; Khare, Anil; Ju, Jing-Yue; Li, Zeng-Min; Duncan, Greg; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 76, # 1-4 p. 139 - 142
反应条件
n-butyllithium; aluminium trichloride; dichlorofluoromethane sulphenyl chloride 1.) ether, hexane, below 25 deg C 2.) ether, 4 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Blackburn, G. Michael; Maciej, Thomas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1935 - 1940
反应条件
n-butyllithium; aluminium trichloride 1.) ether, hexane, below 25 deg C 2.) ether, 4 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Blackburn, G. Michael; Maciej, Thomas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1935 - 1940
反应条件
n-butyllithium; aluminium trichloride 1.) ether, hexane, below 25 deg C 2.) ether, 4 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Blackburn, G. Michael; Maciej, Thomas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1935 - 1940
反应条件
potassium fluoride; 18-crown-6 ether in acetonitrile T=60°C; 168 h;
参考文献
Hutchinson, D. W.; Semple, G.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 21, p. 1 - 4
