3,3-二氯-1-苯基-2-丙烯-1-酮合成路线 （共 8 条）
参考文献
Julia
Annales de Chimie (Cachan, France), 1950 , vol. <12> 5, p. 595,639
反应条件
sodium hydroxide in benzene
Heating;
参考文献
Spitzner, Roland; Menzel, Manfred; Schroth, Werner
Synthesis, 1982 , # 3 p. 206 - 210
参考文献
Levkovskaya, G.G.; Mirskova, A.N.; Kalikhman, I.D.; Voronkov, M.G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 575 - 579
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 634 - 638
反应条件
1: 92 percent / acetonitrile / 0.5 h / -45 °C
2: 85 percent / Triethylamin / benzene; toluene / 1.) 1 h, -20 degC, 2.) 3 h, room temp.
View Scheme
参考文献
Schroth, Werner; Spitzner, Roland; Hugo, Sepp
Synthesis, 1982 , # 3 p. 199 - 203
反应条件
2-(1,3-dithiol-2-ylidene)malononitrile sodium salt in ethanol
3 h; Ambient temperature;
参考文献
Komarova, E. N.; Dmitriev, L. B.; Drozd, V. N.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 10 p. 1811 - 1818
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 10 p. 2097 - 2106
参考文献
Levkovskaya; Bozhenkov; Larina; Mirskova
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 10 p. 1501 - 1506
参考文献
Schroth,W. et al.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1974 , vol. 14, p. 52 - 53
反应条件
boron trifluoride diethyl etherate in chloroform
12 h; Ambient temperature;
参考文献
Schroth, Werner; Burkhardt, Udo; Thiess, Peter; Spitzner, Roland
Zeitschrift fuer Chemie (Stuttgart, Germany), 1984 , vol. 24, # 12 p. 435 - 436
