5-溴-2,3-二羟基苯甲酸甲酯合成路线 (共 3 条)
反应条件
sulfuric acid 16 h; Heating;
参考文献
Yee, Nathan K.; Nummy, Larry J.; Roth, Gregory P.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 19 p. 2279 - 2280
反应条件
1: 71 percent / Br2, HOAc / 20 h / Ambient temperature 2: 84 percent / H2SO4 / 16 h / Heating View Scheme
参考文献
Ellermann, Manuel; Paulini, Ralph; Jakob-Roetne, Roland; Lerner, Christian; Borroni, Edilio; Roth, Doris; Ehler, Andreas; Schweizer, W. Bernd; Schlatter, Daniel; Rudolph, Markus G.; Diederich, Francois
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6369 - 6381
反应条件
T=160°C; 0.666667 h;
参考文献
Diederich, Francois; Jakob-Roetne, Roland; Lerner, Christian; Paulini, Ralph
Patent: US2005/137162 A1, 2005 ;
Location in patent: Page/Page column 6; 10-11; 13 ;